Single crystal diffraction system with microfocus rotating anode generator

Crystal structure determination for macromolecules and chemicals

XtaLAB Synergy-R

The XtaLAB Synergy-R is the most powerful microfocus diffractometer available, combining components to allow you to collect high quality diffraction data. Moreover, the XtaLab Synergy-R offers a number of design features that extend the experimental flexibility to address the most challenging samples.

The XtaLAB Synergy-R system is a tightly integrated instrument with four basic areas of technology: a high-flux, low-maintenance PhotonJet-R X-ray source with continuously variable divergence slit, a high-precision kappa goniometer and Rigaku’s Hybrid Photon Counting detector (HPC) the HyPix-6000HE with extremely low noise and high dynamic range, and the CrysAlisPro software package with sophisticated algorithms to tie the harware together to minimize the time it takes to measure and solve single crystal structures.

Benefits:

  • Fast workflow due to complete integration of software and hardware
  • Extremely high performance due to bright source, noise-free detector and fast goniometer speeds
  • Continuously variable divergence lets you resolve reflections from long unit cells.
  • Compact design to fit in your laboratory
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Features

  • High source flux and increased goniometer speed to allow faster experiments
  • Unique telescopic two-theta arm to reach both longer and shorter crystal-to-detector distances
  • Enhanced kappa goniometer design with symmetrical 2θ positioning
  • Improved X-ray optic alignment mechanism for easy maintenance
  • User-inspired cabinet design for improved workflow
  • New electronically controlled brightness of cabinet and crystal lighting


HyPix-6000HE: Hybrid photon counting detector



Rigaku Oxford Diffraction now offers the HyPix-6000HE Hybrid Photon Counting (HPC) detector. Like all HPCs, the HyPix-6000HE offers direct X-ray photon counting, single pixel point spread function and extremely low noise. The HyPix-6000HE HPC offers a small pixel size of 100 microns, which allows you to better resolve reflections for long unit cells as well as improving reflection profile analysis. The HyPix-6000HE has a high frame rate of 100 Hz, as well as a unique Zero Dead Time mode providing the ultimate in error-free shutterless data collection.

  • Direct photon counting with no phosphor blooming
  • Single pixel point spread function
  • 100 μm x 100 μm pixel size
  • Extremely low noise
  • Frame rate of 100 Hz
  • Electronically gateable
  • Radiation tolerant design



PILATUS3 R 200K: Low maintenance, direct photon counting detector



The PILATUS3 R 200K is a hybrid photon counting (HPC) detector designed to achieve the best possible data quality for diffraction experiments. HPC detectors are direct-detection, single-photon counting devices that have essentially no noise and high sensitivity. Moreover, the high dynamic range excellent DQE characteristics for the PILATUS3 R 200K means that they it is well suited for accurately measuring weak reflections alongside very strong reflections - overload corrections and separate scans for weak and strong data are not necessary. The readout time for the PILATUS3 R 200K is 7 msec readout speed, making it capable of true shutterless data collection, thus removing errors associated with shutter open/close and goniometer start/stop events. HPC detectors have revolutionized the way data are collected at synchrotrons and the PILATUS3 R detectors bring those same capabilities to collect the best possible data at home.
Detector   PILATUS3 R 200K
Active area   83.8 mm x 70.0 mm
Sensor Reverse-biased silicon diode array
Dynamic quantum efficiency (Cu-Kα; Mo-Kα) > 98%; > 76%
Dynamic range 20-bits
Counting rate per pixel 2 x 10⁶ X-ray photons/sec
Readout speed 7 msec
Maximum frame rate 20 Hz
Point-spread function 1 pixel
Cooling Air-cooled
Humidity control Nitrogen or dry air flow
Pixel size 172 μm x 172 μm



PILATUS3 R 300K: Direct photon counting detector with larger active area



The PILATUS3 R 300K is a hybrid photon counting (HPC) detector that is desirable by labs who desire the benefits offered by PILATUS detectors combined with 4-circle goniometers, but prefer a larger active area. HPC detectors are direct-detection, single-photon counting devices that have essentially no noise and high sensitivity. Moreover, the high dynamic range excellent DQE characteristics for the PILATUS3 R 300K means that they it is well suited for accurately measuring weak reflections alongside very strong reflections - overload corrections and separate scans for weak and strong data are not necessary. The readout time for the PILATUS3 R 300K is 7 msec readout speed, making it capable of true shutterless data collection, thus removing errors associated with shutter open/close and goniometer start/stop events. HPC detectors have revolutionized the way data are collected at synchrotrons and the PILATUS3 R detectors bring those same capabilities to collect the best possible data at home.
Detector   PILATUS3 R 300K
Active area   83.8 mm x 106.5 mm
Sensor Reverse-biased silicon diode array
Dynamic quantum efficiency (Cu-Kα; Mo-Kα) > 98%; > 76%
Dynamic range 20-bits
Counting rate per pixel 1 x 10⁷ X-ray photons/sec
Readout speed 7 msec
Maximum frame rate 20 Hz
Point-spread function 1 pixel
Cooling Water-cooled
Humidity control Nitrogen or dry air flow
Pixel size 172 μm x 172 μm
Description
PlateMate

The Rigaku PlateMate is a simple, inexpensive tool for rapid screening of crystals within crystallization plates. The PlateMate supports several different SBS format crystallization plates, though best results are observed using X-ray compatible plates. The PlateMate is quickly installed on Rigaku 4-circle AFC11 partial chi and non-inverted phi goniometers by virtue of the standard IUCr goniometer mount fitting.

(Requires partial chi option for CCD and PILATUS systems. IP systems may require a camera repositioning kit to modify camera angle for proper viewing of crystallization wells)

XtalCheck

The XtalCheck system includes software that facilitates both visual and diffraction imaging of crystallization experiments. With the XtalCheck system, one can easily survey many crystallization experiments by eliminating the need to harvest and cryo-cool samples. Moreover, one can perform serial crystallography experiments, by collecting data from multiple crystals, to achieve complete data sets that can be used for structure solution.

Oxford Cryo 800

The Oxford Cryostream Cooler: The 800 Series Cryostream is the most robust, efficient and user-friendly liquid nitrogen based low temperature system available today. Specific features include a superior laminar flow system, meaning virtually zero risk of icing, extremely quiet running and a fast-start system resulting in a cool-down time to 100K of just 20 minutes.

Oxford Cobra

The Oxford Cobra is the non-liquid nitrogen Cryostream. Combining the efficiency of a Cryostream with the advantages of a non-liquid system, the Cobra offers the ultimate solution for both macromolecular and small molecule crystallography.

Notice: New version of CrysAlisPro v38.46 released on 24th January 2017

We welcome user feedback and CrysAlisPro is frequently updated with new features inspired by users. In this way, our software is continually improving so that your system always provides data of the highest quality. Visit our forum for more information.

User-inspired software for superior data quality
Rigaku Oxford Diffraction systems come complete with CrysAlisPro, our user-inspired data collection and data processing software for macromolecular and small molecule crystallography. . Designed around an easy-to-use graphical user interface, CrysAlisPro can be operated under fully automatic, semi-automatic or manual control.

How to get CrysAlisPro
The software is freely available for users of Rigaku Oxford Diffraction and can be downloaded from our forum. Please register at http://www.rigakuxrayforum.com. Any queries related to the software may be answered on the forum.

Automatic Crystal Screening

At the heart of CrysAlisPro are the automatic crystal screening, data collection and strategy modules. For a typical crystal, a short pre-experiment lasting less than five minutes is recorded to evaluate crystal quality. From the first frame, CrysAlisPro automatically evaluates the crystal quality and provides the user with information regarding the unit cell, intensity estimation by resolution range and suggested frame exposure times for the full data collection.

Fastest Strategy Software

CrysAlisPro‘s sophisticated strategy software automatically calculates the optimal conditions for fast, high quality, complete data collection. All strategies are rapidly calculated based on the specific crystal orientation and unit cell. The user has complete control to optimize the strategy for a wide variety of targets including multiplicity, time and resolution. Strategy calculations are extremely fast and efficient, allowing the user to quickly adapt the data collection conditions for a variety of experiment types.
Automatic and Concurrent Data Reduction

Data reduction and processing initialize automatically with the start of data collection and employ intelligent routines which
tune the parameters to give the best data quality. Processed data are always available and accompanied by real time on-screen feedback of data quality and completeness. CrysAlisPro is programmed for multi-core data processing, meaning rapid results even from the largest data sets.

Software Compatibility
Use CrysAlisPro to import and process diffraction data from synchrotrons and other detector formats. No extra licenses are required. Data files are also easily exported for use in third party data reduction packages including d*TREK, MOSFLM, DENZO and XDS. Reduced data sets can be output in mtz or other data formats for structure solution using other data packages.

Software Updates
We welcome user feedback. CrysAlisPro is frequently updated with new features inspired by users. In this way, the software is continually improving so that your system always provides data of the highest quality. Please visit our forum for more information.

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