In-plane pole figures on a steel sample

In many cases, crystallographic texture (preferred orientation) can be introduced into a material during the fabrication process. For example, when steel sheets are rolled in the manufacturing process, a sheet texture is often produced. Since texture can affect a material's properties by introducing structural anisotropy, it is desirable to measure a material's texture.

The typical measurement to determine texture is called a pole figure. Traditional pole figure measurements are made by recording the intensity of a given Bragg reflection as a function of rotation and tilt of the sample. In an in-plane pole figure, the incident beam, sample rotation, and detector angle are all moved, eliminating the necessity to tilt the sample. The in-plane pole figure also allows a greater range of texture to be recorded, as it now contains the in-plane (sample surface) texture of the sample.

Figure 1 shows an in-plane pole figure of the reflection for a rolled steel sheet sample collected on Rigaku's Ultima IV multipurpose diffraction system. The central dark red portion indicates texture along the [211] direction. The figure shows the pole figure in both in stereographic projection (contour map) and 3D display.

in-plane pole figure

Figure 1



The Ultima IV represents the state-of-the-art in multipurpose X-ray diffraction (XRD) systems. Incorporating Rigaku's patented cross beam optics (CBO) technology for permanently mounted, permanently aligned and user-selectable parallel and focusing geometries, the Ultima IV X-ray diffractometer can perform many different measurements...fast. Read more...

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