R-AXIS SPIDER large area curved imaging plate detector
Finally a small molecule system that is experimentally versatile
and extremely easy and inexpensive to maintain.
The large imaging plate format of the SPIDER provides outstanding
versatility that cannot be matched by CCD-based detectors.
Compare
the SPIDER aperture to the size of a typical CCD
- Routine small molecule analysis is exactly that: routine. The
large aperture and lack of the dark current associated with CCD
detectors, allows rapid and complete data collection on standard
samples. No need to worry about collecting the full resolution of
diffraction since the large aperture automatically collects the
diffraction limit with Mo radiation.
- Absolute configurations of organic molecules could not be
easier. Switch your tube to Cu and the large active area of the detector
provides simultaneous measurement of -60° to +144° in 2θ,
more than enough for a publication quality structure.
- Weak or poorly scattering crystals are easily handled due to a
number of factors. The lack of a dark current (an attribute of any CCD
detector) means that long exposures are not degraded by electronic
noise.
- High quality electron density studies are achieved by a number
of special attributes, specific to imaging plate technology. Error in
measurement is reduced by a lack of dark current. Inter-image scaling
features are reduced because so many more reflections are measured on a
single image as compared to CCD detectors. The high dynamic range of the
imaging plate as compared to CCD detectors provides the ability to
measure weak and strong reflections accurately during the same scan.
- Versatile Experimentation is achieved by a phosphor that is
essentially independent of radiation for Ag, Mo, Cu and Cr. The large
aperture is ideal for measurement of powder samples, diffuse scattering
or other specialized experiments that might be imagined.
- Easy and cheap to maintain. Imaging plates do not require a
detector cooling system, which automatically reduces the device's
overall
complexity. There is no component in a SPIDER (like a CCD chip) that, if
failed, would be catastrophically expensive to replace for someone
without a service contract. As with all Rigaku detectors, Rigaku
manufactures the SPIDER and will support the product long into the
future.
Features
- Compatibility with Rigaku sealed tube and rotating anode sources
- Partial-χ or fixed-χ goniometer options
- Source-to-sample distance: 127.4 mm
- Aperture: 466 mm x 256 mm
- Pixel size: 100 μm x 100 μm
- Read time: 51.2 seconds
- Erase time: 20 seconds
- Over 100 R-AXIS RAPID/SPIDER systems installed since 1998
- Supported by CrystalClear™
and HKL-2000®