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Thermal desorption of aromatic compound in metallic complex

TA-5007: Thermal desorption of aromatic compound in metallic complex

 

It is available of efficient simulation using Dynamic TG for debinding process of ceramic chip capacitor.

The traditional TG-DTA can be measured by controlling temperature with time as parameter which has no relation with sample change, on the other hand, SCTG (Dynamic TG ) can be measured by controlling temperature with sample amount change as parameter. Compared Dynamic TG to traditional TG-DTA, it is available to measure with enhancing the resolution and prompting gradual reaction of sample.

We observed the difference of thermal desorption for 3 benzene molecules which combined in the metallic complex due to the different electrostatic interaction.

Thermal analysis products from Rigaku

TG-DTA is a hyphenated technology generally referred to as simultaneous thermal analysis (STA).

 

 

DSC is a thermal analysis technique that quantifies the amount of energy in a reaction.

Quantifies the energy changes in reactions such as melting, transition, crystallization and glass transition temperature.

DSC8271 is a high-temperature type DSC with a maximum temperature of 1,500°C.

TMA is the measurement of a change in dimension or mechanical property of the sample while it is subjected to a controlled temperature program.

 

The compact humidity generator (HUM-1) is connected to the TG-DTA for measurements under constant relative humidity water vapor atmosphere.

 

TMA/HUM measures change in dimension or mechanical property of a sample while subjected to a temperature regime under water vapor atmosphere with a constant relative humidity.

Thermo Mass Photo combines simultaneous thermal analysis with mass spectrometry. This technique is suitable for the qualitative analysis of  evolved gases coincident with the STA signal.

In TG-FTIR, gases evolved by volatilization or thermal decomposition are qualitatively analyzed, which allows you to track changes in the generated amount along with the temperature change.