Difractómetro de rayos X con microfoco único o dual para todas sus necesidades de cristalografía
Un sistema rápido y ágil para el análisis en 3D de pequeña molécula/H2>
XtaLAB Synergy-S
Pensando en su éxito, hemos producido el difractómetro XtaLAB Synergy-S para la difracción de rayos X de monocristal. Con una combinación de componentes de punta y un software inspirado en el usuario; vinculados por medio de una arquitectura altamente paralelizada, el XtaLAB Synergy-S produce datos rápidos y precisos de una manera inteligente.
El sistema se basa en nuestra nueva serie de fuentes de microfoco PhotonJet-S. Esta tercera generación de fuentes ha sido diseñada para maximizar los fotones de rayos X en la muestra mediante el uso de una combinación de nuevas ópticas, nuevos tubos más duraderos, y un sistema de alineación mejorada. Los PhotonJets están disponibles en longitudes de onda Cu, Mo o Ag, ya sea en una configuración de fuente única o doble.
El nuevo goniómetro kappa ha sido completamente rediseñado para incorporar una mayor velocidad de motor y un brazo telescópico único de dos thetas para proporcionar una flexibilidad total en su experimento de difracción. El goniómetro es compatible con la más amplia variedad de detectores para satisfacer sus necesidades. CCD o HPC? Usted elije.
Beneficios:
- Mejora significativa en la calidad y la velocidad de la recolección de datos sobre los anteriores sistemas de microfoco de tubo sellado.
- Una distancia del detección más larga o más corta significa que se puede analizar una variedad más amplia de muestras con una precisión excepcional.
- Mínimo tiempo de inactividad con tubo de rayos X de larga duración, compatible con diagnósticos y solución de problemas en línea.

Features
- Fuente de alto flujo y aumento de la velocidad del goniómetro para permitir experimentos más ágiles y rápidos.
- Telescópico único de brazo dos thetas para llegar a distancias largas y cortas de cristal a detector.
- Diseño de goniómetro kappa mejorado con posicionamiento simétrico 2θ.
- Nueva fuente de alto flujo con tubos de rayos X de más larga duración.
- Mecanismo de alineamiento óptico de rayos X mejorado para un fácil mantenimiento.
- La más amplia variedad de detectores disponibles: HPC o CCD
- Caja de diseño inspirado en el usuario para un mejor flujo de trabajo
- Nueva iluminación de la caja y del cristal controlada electrónicamente.
This video shows the XtaLAB Synergy-S single crystal X-ray diffractometer in action. Watch the fast diffractometer race the Rigaku office coffee machine to obtain a the X-ray crystal structure; this system is fast!
HyPix-6000HE: Hybrid photon counting X-ray detector

Rigaku Oxford Diffraction now offers the HyPix-6000HE Hybrid Photon Counting (HPC) X-ray detector. Like all HPCs, the HyPix-6000HE offers direct X-ray photon counting, single pixel point spread function and extremely low noise. The HyPix-6000HE HPC offers a small pixel size of 100 microns, which allows you to better resolve reflections for long unit cells as well as improving reflection profile analysis. The HyPix-6000HE has a high frame rate of 100 Hz, as well as a unique Zero Dead Time mode providing the ultimate in error-free shutterless data collection.
Detector | HyPix-6000HE | |
Active area | 77.5 mm x 80.0 mm | |
Dynamic quantum efficiency (Cu-Kα) | > 98% | |
Dynamic range | 31-bits | |
Counting rate per pixel | 1 x 10⁶ X-ray photons/sec | |
Readout speed | 0 ms in ZeroDeadTime mode | |
Maximum frame rate | 100 Hz | |
Point-spread function | 1 pixel | |
Cooling | Air-cooled | |
Humidity control | Not required | |
Pixel size | 100 μm x 100 μm |
HyPix-Arc 150°: Curved photon counting X-ray detector

The HyPix-Arc 150° is a unique, curved Hybrid Photon Counting (HPC) X-ray detector for single crystal diffraction applications. HyPix-Arc 150° has the highest 2θ range at a single position available for the home lab.
Collect more data in a single exposure with less reflection profile distortion:
The HyPix-Arc 150° offers 150 degrees angular coverage from edge to edge. This is more than enough to collect complete single crystal diffraction data, according to IUCr guidelines, for even Cu Kα X-ray wavelength from a single theta position. High and low angle data are measured at the same time, under the same conditions for better scaling, faster data and reduced dose time.
A curved detector minimizes peak distortion by ensuring that, even at short crystal-to-detector distances, diffracted beams are closer to perpendicular than is possible with a flat geometry.
Features:
- Lowest reflection profile distortion
- Faster data collection
- Higher 2θ coverage in a single image
- All reflections measured under the same conditions
- Capture more diffracted photons per exposure
PILATUS3 R 200K: Low maintenance, direct photon counting X-ray detector

The PILATUS3 R 200K is a hybrid photon counting (HPC) X-ray detector designed to achieve the best possible data quality for diffraction experiments. HPC detectors are direct-detection, single-photon counting devices that have essentially no noise and high sensitivity. Moreover, the high dynamic range excellent DQE characteristics for the PILATUS3 R 200K means that they it is well suited for accurately measuring weak reflections alongside very strong reflections - overload corrections and separate scans for weak and strong data are not necessary. The readout time for the PILATUS3 R 200K is 7 msec readout speed, making it capable of true shutterless data collection, thus removing errors associated with shutter open/close and goniometer start/stop events. HPC X-ray detectors have revolutionized the way data are collected at synchrotrons and the PILATUS3 R detectors bring those same capabilities to collect the best possible data at home.
Detector | PILATUS3 R 200K | |
Active area | 83.8 mm x 70.0 mm | |
Sensor | Reverse-biased silicon diode array | |
Dynamic quantum efficiency (Cu-Kα; Mo-Kα) | > 98%; > 76% | |
Dynamic range | 20-bits | |
Counting rate per pixel | 2 x 10⁶ X-ray photons/sec | |
Readout speed | 7 msec | |
Maximum frame rate | 20 Hz | |
Point-spread function | 1 pixel | |
Cooling | Air-cooled | |
Humidity control | Nitrogen or dry air flow | |
Pixel size | 172 μm x 172 μm |
PILATUS3 R 300K: Direct photon counting X-ray detector with larger active area

The PILATUS3 R 300K is a hybrid photon counting (HPC) X-ray detector that is desirable by labs who desire the benefits offered by PILATUS detectors combined with 4-circle goniometers, but prefer a larger active area. HPC detectors are direct-detection, single-photon counting devices that have essentially no noise and high sensitivity. Moreover, the high dynamic range excellent DQE characteristics for the PILATUS3 R 300K means that they it is well suited for accurately measuring weak reflections alongside very strong reflections - overload corrections and separate scans for weak and strong data are not necessary. The readout time for the PILATUS3 R 300K is 7 msec readout speed, making it capable of true shutterless data collection, thus removing errors associated with shutter open/close and goniometer start/stop events. HPC X-ray detectors have revolutionized the way data are collected at synchrotrons and the PILATUS3 R detectors bring those same capabilities to collect the best possible data at home.
Detector | PILATUS3 R 300K | |
Active area | 83.8 mm x 106.5 mm | |
Sensor | Reverse-biased silicon diode array | |
Dynamic quantum efficiency (Cu-Kα; Mo-Kα) | > 98%; > 76% | |
Dynamic range | 20-bits | |
Counting rate per pixel | 1 x 10⁷ X-ray photons/sec | |
Readout speed | 7 msec | |
Maximum frame rate | 20 Hz | |
Point-spread function | 1 pixel | |
Cooling | Water-cooled | |
Humidity control | Nitrogen or dry air flow | |
Pixel size | 172 μm x 172 μm |
XtaLAB Synergy accessories
Description | ||
---|---|---|
Oxford Cryo 800 |
El Oxford Cryostream Cooler: La serie Cryostream 800 es el sistema de baja temperatura a base de nitrógeno líquido más resistente, eficiente y fácil de usar disponible hoy en día. Las características específicas incluyen un sistema de flujo laminar superior, es decir, prácticamente cero riesgo de formación de hielo, extremadamente silencioso y un sistema de inicio rápido que resulta en un tiempo de enfriamiento de 100K de sólo 20 minutos |
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CrysAlisPro v40
Now with full 64 bit compatibility!
Rigaku Oxford Diffraction single crystal X-ray diffractometers come complete with CrysAlisPro, our user-inspired data collection and data processing software for small molecule and protein crystallography. Designed around an easy-to-use graphical user interface, CrysAlisPro can be operated under fully automatic, semi-automatic or manual control.

The latest release, CrysAlisPro v.40, is now fully 64 bit compatible and ready for the future. As modern diffractometers increase in performance and speed, your experiments generate bigger and bigger images and datasets. Additionally, supporting large detectors with very high pixel counts, such as those more commonly found at synchrotrons, requires large amounts of memory. Moving to 64 bit gives applications access to more memory, enabling the handling of these very large image sizes and data sets.
Expanded support for older Rigaku instrumentation and third party hardware is also in this release.
See below for other new software features that have recently been introduced.
How to get CrysAlisPro
The software is freely available for users of Rigaku Oxford Diffraction single crystal X-ray instruments and can be downloaded from our forum. Please register at http://www.rigakuxrayforum.com. Any queries related to the software may be answered on the forum.
CrysAlisPro: Seamless from start to finish
CrysAlisPro combines automated crystal screening, the fastest and most accurate strategy software available, concurrent data reduction and automatic small molecule structure solution. Visual feedback is provided for each step with clear, color-coded guidance so that both novices and experts can collect high-quality data in the shortest time possible.
CrysAlisPro is built on a command line interface and the GUI retains full manual control options for those that want them. It is your choice how to analyse your data.
CrysAlisPro processes data using sophisticated algorithms to provide the highest quality data. As technology or approaches change, our software team incorporates these to further advance data analysis and processing.

Processing of challenging and non-standard data collections
CrysAlisPro contains a comprehensive and highly effective range of tools for tackling a wide range of samples from easy to challenging, and non-standard crystal samples. For example, EwaldExplorer and Ewald 3D (NEW!) easily identify effects, problems or artifacts in difficult or problematic datasets.
Ewald3D allows visualization of measured reciprocal space in 3-dimensions and in an undistorted way. Identifying diffuse scatter, modulation, subtle twinning, or incorrect instrument models is quick and easy with this brand new feature.
Supporting a range of crystallographic setups and applications
In addition to standard data collection routines, CrysAlisPro contains tools for working with non-standard experimental setups and sample types, including:
- High pressure data collections
- Variable temperature and multi-wavelength experiments
- Powder experiments (data collection and processing)
- Automatic screening or full data collections of several in situ protein crystals
- Highly absorbing samples
- Up to 8-fold twinned samples
- Charge density measurements
- Absolute structure determination
Software Compatibility
Exporting frames or data from CrysAlisPro into suitable alternative formats such as mosFLM, XDS, Denzo (HKL 2000) or another Esperanto format is easily achieved. Use CrysAlisPro’s data collection strategy to achieve the best data coverage in the quickest possible time and then automatically output into HKLF format for small molecule datasets or into the MTZ format for protein datasets.
CrysAlisPro is used by numerous research groups to process their synchrotron data. Our software is capable of importing data from several different detector types; known or unknown.
AutoChem
AutoChem is the ultimate productivity tool for small molecule chemists, offering fast, fully automatic structure solution and refinement during data collection. Developed in collaboration with OlexSys Ltd (Durham University, UK), AutoChem works in conjunction with Olex2 where more advanced structure solution and refinement functionality exists. AutoChem is seamlessly integrated within CrysAlisPro, and forms an integral part of our ‘What is this?’ feature.
The ‘What is this?’ feature gives you structures in seconds and ensures you are not wasting time collecting full datasets on known samples or starting materials. It is an alternative pre-experiment option, which is used to plan your full data collections.

Papers published using the XtaLAB Synergy-S
- Lin Lim F P, Tan K C, Luna G, Tiekink E R T, Dolzhenko A V. “ A new practical synthesis of 3-amino-substituted 5-aminopyrazoles and their tautomerism.” Tetrahedron (2019), 75(15): 2314-2321. https://www.sciencedirect.com/science/article/pii/S0040402019302625
- Wiscons R A, Coropceanu V, Matzger A J. “Quaternary Charge-Transfer Solid Solutions: Electronic Tunability through Stoichiometry.” Chem. Mater. (2019), available online 13 March https://pubs.acs.org/doi/abs/10.1021/acs.chemmater.9b00502
- Takahashi Y, Uehara T, Matsuhashi C, Yamaji M, Mutai T, Yoshikawa I, Houjou H, Kitagawa K, Suenobu T, Maki S, Hirano T. “Spectroscopic properties of push-pull 2-(4-carboxyphenyl)-6-dimethylaminobenzothiazole derivatives in solution and the solid state.” J. Photochem. Photobio. A:Chem. (2019), 376: 324-332. https://www.sciencedirect.com/science/article/abs/pii/S1010603019301613
- Konkankit C C, Vaughn B A, MacMillan S N, Boros E, Wilson J J. “Combinatorial Synthesis to Identify a Potent, Necrosis-Inducing Rhenium Anticancer Agent.” Inorg. Chem. (2019), available online 22 Feb https://pubs.acs.org/doi/abs/10.1021/acs.inorgchem.8b03552
- King A P, Gellineau H A, MacMilan S N, Wilson J J. “Physical properties, ligand substitution reactions, and biological activity of Co (III)-Schiff base complexes.” Dalton Transactions (2019), just accepted 11 Jan. https://pubs.rsc.org/en/content/articlelanding/2019/dt/c8dt04606a/unauth...
- Grey I E, Mumme W G, Downes P J, Grguric B A, Gable R W. “Segelerite from the mount Deverell variscite deposit, Western Australia. Hydrogen bonding and relationship to jahnsite.” European Journal of Mineralogy (2019), available online 10 Jan https://www.ingentaconnect.com/content/schweiz/ejm/pre-prints/content-ej...
- Malmberg R, Bachmann M, Blacque O, Venkatesan K. “Thermally Robust and Tunable Phosphorescent Gold(III) Complexes Bearing (N^N)-type Bidendates as Ancillary Chelates.” Chemistry – A European Journal (2019), available online 7 Jan https://onlinelibrary.wiley.com/doi/abs/10.1002/chem.201805486
- Tan Y J, Tan Y S Yeo C I Chew J, Tiekink E R T. “In vitro anti-bacterial and time kill evaluation of binuclear tricyclohexylphosphanesilver(I) dithiocarbamates, {Cy3PAg(S2CNRR’)}2.” J. Inorg. Chem. (2019) 192: 107-118 https://www.sciencedirect.com/science/article/pii/S016201341830535X
- Ali M O, Lasseter J C, Żurawiński R, Pietrzak A, Pecyna J, Wojciechowski J, Friedli A C, Pociecha D, Kaszyński P. “Thermal and Photophysical Properties of Highly Quadrupolar Liquid-Crystalline Derivatives of the [closo-B12H12]2- Anion.” Chemistry – A European Journal (2018) just published 17 December https://onlinelibrary.wiley.com/doi/full/10.1002/chem.201805392
- Zhen J, Zhou W, Chen M, Li B, Jia L, Wang M, Yang S. “Pyridine-functionalized fullerene additive enabling coordination interactions with CH3NH3PbI3 perovskite towards highly efficient bulk heterojunction solar cells.” Journal of Materials Chemistry A (2019), 7: 2754-2763 https://pubs.rsc.org/en/content/articlelanding/2019/ta/c8ta12206g/unauth...
- Fu J, Ren Z, Bacsa J, Musaev D G, Davies H M L. “Desymmetrization of cyclohexanes by site- and stereoselective C-H functionalization.” Nature Letters (2018), 564: 395-399 https://www.nature.com/articles/s41586-018-0799-2#Sec4
- Akagi S, Horiguchi T, Fujii S, Kitamura N. “Terminal Ligand (L) Effects on Zero-Magnetic-Field Splitting in the Excited Triplet States of [{Mo6Br8}L6]2- (L= Aromatic carboxylates).” Inorg. Chem. (2019), 58(1): 703-714 https://pubs.acs.org/doi/abs/10.1021/acs.inorgchem.8b02881
- Molcanov K, Jelsch C, Landeros B, Hernández-Trujilo J, Wenger E, Stilinović V, Kojic-Prodic B, Escudero-Adán E C. “Partially covalent two-electron/multicentric bonding between semiquinone radicals.” Cryst. Growth Des. (2019) 19: 391-402 https://pubs.acs.org/doi/abs/10.1021/acs.cgd.8b01484
- Ogawa A, Oohora A, Hayashi T. “Synthesis and Characterization of meso-Substituted Cobalt Tetrahydrocorrin and Evaluation of its Electrocatalytic Behavior Toward CO2 Reduction and H2 Evolution.” Inorg. Chem. (2018) 57(23): 14644-14652 https://pubs.acs.org/doi/full/10.1021/acs.inorgchem.8b02333
- Yang Y, Zhang S-S, Zhao Q-Q, Wang X-P, Tung C-H, Sun D. “Construction of Crystalline One-Dimensional Infinite Argentophilic Silver Alkynyl Assemblies and their Luminescence Properties.” Eur. J. Inorg. Chem. (2018), 47 https://onlinelibrary.wiley.com/doi/abs/10.1002/ejic.201800998
- Lipowska M, Klenc J, Taylor A T, Marzilli L G. “fac-99m Tc/Re-tricarbonyl complexes with tridendate aminocarboxyphosphonate ligands: suitability of the phosphonate group in chelate ligand design of new imaging agents.” Inorg. Chim. Acta (2019) 486: 529-537 https://www.sciencedirect.com/science/article/pii/S0020169318314464
- Gradstein F M, Waskowska A, Kopaevich L, Watkins D K, Friis H, Pérez Panera J. “Berriasian planktonic foraminifera and calcareous nannofossils from Crimea Mountains, with reference to microfossil evolution.” Swiss Journal of Palaeontology (2018), published online 7 November https://link.springer.com/content/pdf/10.1007%2Fs13358-018-0175-8.pdf
- Alexandropoulos D I, Alaimo A A, Sun D, Stamatatos T C. “A New {Dy5} Single-Molecule Magnetic Bearing the Schiff Base Ligand N-Naphthalidene-2-amino-5-chlorophenol.” Magnetochemistry (2018) 4(4): 48 https://doi.org/10.3390/magnetochemistry4040048
- Getmanenko Y A, Mullins C S, Nesterov V N, Lake S, Risko C, Johnston-Halperin E. “Magnetic ordering in a vanadium-organic coordination polymer using a pyrrolo[2,3-d:5,4-d’]bis(thiazole)-based ligand.” RSC Adv. (2018) 8: 36223-36232 https://pubs.rsc.org/en/content/articlehtml/2018/ra/c8ra05697h
- Worrell A, Sun D, Mayans J, Lampropoulous C, Escuer A, Stamatatos T C. “Oximato-Based Ligands in 3d/4f-Metal Cluster Chemistry: A Family of {Cu3Ln} Complexes with a “Propeller”-like Topology and Single-Molecule Magnetic Behavior.” Inorg. Chem. (2018) 57(21): 13944-13952 https://pubs.acs.org/doi/ipdf/10.1021/acs.inorgchem.8b02495
- VanGelder L E, Petel B E, Nachtigall O, Martinez G, Brennessel W W, Matson E M. “Organic Functionalization of Polyoxovanadate-alkoxide Clusters: Improving the Solubility of Multimetallic Charge Carriers for Nonaqueous Redox Flow Batteries.” ChemSusChem (2018), first published 15 Oct https://onlinelibrary.wiley.com/doi/pdf/10.1002/cssc.201802029
- Tan Y S, Chun, H Z, Jotani M M, Tiekink E R T. “Steric control of supramolecular association in structures of Zn(S2COR)2 with N,N’-bis(pyridine-4ylmethyl)oxalamide.” Z. Kristallogr. Cryst. Mater. (2018), first published 8 Oct https://doi.org/10.1515/zkri-2018-2120
- Pejić J, Vušak D, Szalontai G, Prugovečki B, Mrvoš-Sermek D, Matković-Čalogović D, Sabolović J. “Disorder at the Chiral Cα Center and Room Temperature Solid-State cis-trans Isomerization; Synthesis and Structural Characterization of Copper(II) Complexes with D-allo, L-Isoleucine.” Crys. Growth Des. (2018) 18(9): 5138-5154 https://pubs.acs.org/doi/abs/10.1021/acs.cgd.8b00589
- Siu J C, Sauer G S, Saha A, Macey R L, Fu N, Chauviré T, Lancaster K M, Lin S. “Electrochemical Azidooxygenation of Alkenes Mediated by a TEMPO-N3 Charge-Transfer Complex.” J. Am. Chem. Soc. (2018) 140(39): 12511-12520 https://pubs.acs.org/doi/10.1021/jacs.8b06744
- Kadassery K J, MacMillan S N, Lacy D C. “Biphosphine phenol and phenolate complexes of Mn (I): manganese(I) catalyzed Tishchenko reaction.” Dalton Transactions (2018) 47: 12652-12655 https://pubs.rsc.org/en/content/articlelanding/2018/dt/c8dt02933d#!divAb...
- Stone I B, Jermaks J, MacMillan S N, Lambert T H. “The Hydrazine-O2 Redox Couple as a Platform for Organocatalytic Oxidation: Benzo[c]cinnoline-Catalyzed Oxidation of Alkyl Halides to Aldehydes.” Angew. Chem. Int. Ed. (2018) 57(38) https://onlinelibrary.wiley.com/doi/abs/10.1002/anie.201807134
- Meyer R L, Brennessel W W, Matson E M. “Synthesis of a gallium-functionalised polyoxovanadate-alkoxide cluster: Toward a general route for a heterometal installation.” Polyhedron (2018), 156: 303-311 https://www.sciencedirect.com/science/article/pii/S027753871830576X?via%...
- Ravat P, Šolomek T, Häussinger D, Blacque O, Juríček M. “Dimethylcethrene: A Chiroptical Diradicaloid Photswitch.” J. Am.. Chem Soc. (2018) 140: 10839 – 10847 https://pubs.acs.org/doi/pdf/10.1021/jacs.8b05465
- Shapiro J A, Morrison K R, Chodisetty S S, Musaev D G, Wuest W M. “Biologically Inspired Total Synthesis of Ulbactin F, an Iron-Binding Natural Product.” Org. Lett. (2018), 20(18): 5922-5926 https://pubs.acs.org/doi/abs/10.1021/acs.orglett.8b02599
- Zhao C, Schwartz T, Stöger B, White F J, Chen J, Ma D, Fröhlich J, Kautny P. “Controlling excimer formation in indolo[3,2,1-jk]carbazole/9H-carbazole based host materials for RGB PhOLEDs” J. Mat. Chem. C. (2018), 6: 9914-9924 https://pubs.rsc.org/en/content/articlepdf/2018/tc/c8tc03537g
- Movassaghi S, Leung E, Hanif M, Lee B Y T, Holtkamp H U, Tu J K Y, Söhnel T, Jamieson S M F, Hartinger C G. “A Bioactive L-Phenylalanine-Derived Arene in Miltitargeted Organoruthenium Compounds: Impact on the Antiproliferative Activity and Mode of Action” Inorg. Chem (2018) 57(14): 8521-8529 https://pubs.acs.org/doi/abs/10.1021/acs.inorgchem.8b01187
- Su Y, Su H-F, Wang Z, Li Y, Schein S, Zhao Q, Wang X, Tung C-H, Sun D. “Three Silver Nests Capped by Thiolate/Phenylphosphonate.” Chemistry:A European Journal (2018), 24(56): 15096-15103 https://onlinelibrary.wiley.com/doi/abs/10.1002/chem.201803203
- Wu Y, Halat D M, Wei F, Binford T, Seymour I D, Gaultois M W, Shaker S, Wang J, Grey C P, Cheetham A K. “Mixed X-site formate-hypophosphite hybrid perovskites.” Chemistry: A European Journal (2018), 24(44): 11309-11313 https://onlinelibrary.wiley.com/doi/abs/10.1002/chem.201803061
- Morgan M T, Yang B, Harankhedkar S, Nabatilan A, Bourassa D, McCallum A M, Sun F, Wu R, Forest C R, Fahrni C J. “Stabilization of aliphatic phosphines by auxillary phosphine sulfides offers zeptomolar affinity and unprecedented selectivity for probing biological Cu(II).” Angew. Chem (2018) 130(31): 9859-9863 https://onlinelibrary.wiley.com/doi/abs/10.1002/ange.201804072
- Scholl K, Dillashaw J, Timpy E, Lam Y, DeRatt L, Benton T R, Powell J P, Houk K N Morgan J M. “Quinine-Promoted, Enantioselective Boron-Tethered Diels-Alder Reaction by Anomeric Control of Transition-State Conformation.” J. Org Chem. (2018) 83: 5756-5765 https://pubs.acs.org/doi/abs/10.1021/acs.joc.8b00938
- Akondi S M, Gangireddy P, Pickel T C, Liebeskind L S. “Aerobic, Diselenide-Catalyzed Redox Dehydration: Amides and Peptides.” Org. Lett. (2018) 20: 538-541 https://pubs.acs.org/doi/10.1021/acs.orglett.7b03620
- Cundari T R, Jacobs B P, MacMillan S N, Wolczanski P T. “Dispersion forces play a role in (Me2IPr)Fe(=NAd)R2 (Ad = adamantly; R=neoPe, 1-nor) insertions and Fe-R bond dissociation enthalpies (BDEs)” Dalton Transactions (2018) 47: 6025-6030 http://pubs.rsc.org/en/Content/ArticleLanding/2018/DT/C7DT04145D#!divAbs...
- Vaccarello D N, O’Connor K S, Iacono P, Rose J M, Cherian A E, Coates G W. “Synthesis of Semicrystalline Plyolefin Materials: Precision Methyl Branching via Stereoretentive Chain Walking.” J. Am. Chem. Soc. (2018) 140(20): 6208-6211 https://pubs.acs.org/doi/10.1021/jacs.8b02963
- Molčanov K, Mou Z, Kertesz M, Kojić-Prodić B, Stalke D, Demeshko S, Šantić A, Stilinović. “Two-electron / multicenter – pancake bonding in π-stacked trimers in a salt of tetrachloroquinone anion.” Chemistry: A European Journal, (2018) 24(33): 8292-8297 https://onlinelibrary.wiley.com/doi/pdf/10.1002/chem.201800672
- Milić J, Zalibera M, Talaat D, Nomrowski J, Trapp N, Ruhlmann L, Boudon C, Wenger O S, Savitsky A, Lubitz W, Diederich F. “Photoredox-Switchable Resorcin[4]arene Cavitands: Radical Control of Molecular Gripping Machinery via Hydrogen Bonding.” Chemistry: A European Journal, (2017) 24(6): 1431-1440 https://onlinelibrary.wiley.com/doi/abs/10.1002/chem.201704788
- Haberland S, Finke A D, Kerisit N, Katan C, Trolez Y, Gawel P, Leito I, Lõkov M, Järviste R, Kaupmees K, Trapp N, Ruhlmann L, Boudon C, Himmel D, Diederich F. “Enhancement of Push-Pull Properties of Pentafulvene and Pentafulvene Derivatives by Protonation at Carbon.” Eur J. Org. Chem., (2018) 6:739-749 https://onlinelibrary.wiley.com/doi/abs/10.1002/ejoc.201800039
- Hao W, Harenberg J H, Wu X, MacMilan S N, Lin S. “Diastereo- and Entatioselective Formal [3 + 2] Cycloaddition of Cyclopropyl Ketones and Alkenes via Ti-Catalyzed radical Redox Relay” J. Am. Chem. Soc. (2018) 140(10): 3514-3517 https://pubs.acs.org/doi/10.1021/jacs.7b13710
- Ye K-Y, Pombar G, Fu N, Sauer G S, Keresztes I, Lin S. “Anodically Coupled Electrolysis for the Heterodifunctionalization of Alkenes.” J. Am. Chem. Soc. (2018) 140(7): 2438-2441 https://pubs.acs.org/doi/10.1021/jacs.7b13387
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ELement ANalyzer
Elemental analysis attachment for single crystals
The ELement ANalyzer is a state-of-the-art attachment that allows us to obtain qualitative information on elements in a single crystal at the same time as X-ray diffraction data collection for a single crystal structural analysis. By measuring the X-ray fluorescence spectrum emitted during X-ray diffraction experiments with the ELement ANalyzer, it becomes possible to perform elemental analysis on a single grain of crystal. The ELement ANalyzer can be used for confirmation the presence of central metal(s) in a mononuclear or polynuclear complex or solvent in a crystal for small molecule X-ray crystallography. There is a broad range of possible applications of the ELement ANalyzer in scientific fields.