|Course Name:||ZSX Primus IV & Supermini200 training|
|Sessions:||14-16 February, 2022
12-14 September, 2022
5-7 December, 2022
|Course Times:||9 a.m. – 4 p.m. (CET)|
The trainings focus on the practical use of Rigaku spectrometers and software. The sessions will mainly take place at the instrument and well selected examples and exercises will be used to make you familiar with basic principles and functionality.
The courses give an overview of the ZSX Software, cover on the one hand the standardless SQX-Analysis and approaches to refining SQX results. On the other hand, strategies are explained how to develop quantitative analysis methods (calibrations) considering the respective analytical situation (line overlaps, matrix & preparation effects etc.).
Depending on the participants’ analytical requirements, special topics will be explained during the course on request (e.g. spot analysis & mapping, thin film, filters etc.)
Topics like PHA adjustment, drift correction, monitoring the instrument and performing control measurements will be discussed. Utilities and additional software functions (chemical compounds, data backup…) are shown as well.
Who Should Attend
Chemists, Operators, Engineers, Research Scientists and University Students in University and Operators of the XRF spectrometers supplied by Rigaku.
How to Join
Registration is required. The number of places is limited.
An email with the details and online training link will be sent to registered attendees prior to the training course.
Persons attending the training are advised to have a personal computer with ZSX Guidance software installed and the software dongle/network license that is required to run the software.
Course Agenda - Lunch (1 hour) is at 12 noon
|9:00 – 12:00||1. Welcome and Introduction|
|2. XRF Theory of X ray Physics|
|3. The X-ray Spectrometer configuration|
|4. Overview ZSX Guidance software|
|13:00 – 16:00||
5. Sample preparation
|9:00 – 12:00||1. Introduction to Standardless SQX analysis|
| a) Qualitative SQX analysis
b) Fixed angle mode
c) Matching library
d) SQX Scatter FP
e) Library sensitivities
|13:00 – 16:00||2. Quantitative analysis|
|a) Setting up an Empirical Calibration Part 1|
|b) Standards available only one type to be chosen
CRM STD wide oxide range FB
Clay Pressed powder
|c) Optimization of measuring conditions|
|d) Background fitting|
|3. Setting up an Empirical Calibration Part 2
a) Calibration coefficient regression graphs
b) Overlap corrections / Theoretical alpha corrections
|4. Drift corrections|
|5. Calibration Check sample, Stability check and daily check sample|
|9:00 – 12:00||1) Setting up an Empirical Calibration Part 3|
|2) Verification and Validation of the method|
3) Setting up process parameters in the calibration
|13:00 – 16:00||4) Data Evaluation|
|5) Maintenance of the Instrument|
|6) Maintenance of calibration|
|7) Evaluation of the training|
|8) Conclusion and closing|
Note: During training course, the latest version of software for instrument control and analysis software that is available on the market is used. Therefore, details of the operation might be different from your environment. Our trainers are more than happy to discuss the operations on your version of the software.
The training program is prepared to fit online format. If the travel situation improves the training may take place at Rigaku Europe SE laboratory as on-site format or as hybrid format. Appropriate change in the program will be then communicated to participants.