Sho Ito and Akihito Yamano
3D electron diffraction (3D ED)/Micro electron diffraction (MicroED) is a technique that can provide measurers with three-dimensional molecular structures from crystals of submicron order. However, 3D ED/Micro ED requires expertise in both electron microscopy and crystallography. Here, we introduce the newly developed electron diffractometer XtaLAB Synergy-ED specialized for 3D ED/MicroED experiments, its instrument configuration, measurement flow, and measurement examples.