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XtaLAB Synergy-S
Benefits
  • Fast, accurate data collection due to high-speed kappa goniometer, high-flux X-ray source, fast, low-noise X-ray detector, and highly optimized instrument control software.
  • Enhanced experimental versatility when the dual-source option is selected from three possible wavelengths (Mo, Cu, or Ag).
  • Highest level of user safety with multiply redundant electromechanical safety circuits built into the ergonomically designed radiation enclosure.
  • Minimize your downtime by utilizing built-in online diagnostics and troubleshooting to diagnose and fix almost all problems without a site visit.
  • Automatically solve structures and determine what your sample is in a few seconds before committing to a full dataset by using the “What is this?” feature.
  • Improve your ability to investigate small samples because the solid state pixel array technology of the HyPix X-ray detectors means that X-ray photons are counted instantaneously as they arrive at the detector. There is no conversion to visible light by a scintillator so the energy of the photon can be assessed at moment of detection leading to essentially noise free images. And noise-free images means you can count longer for weakly diffracting crystals without a loss in data quality arising from detector noise.
  • Optimize data collection speed when you select the optional HyPix-Arc 100° or HyPix-Arc 150° curved detectors, which allow theta coverage exceeding the largest detectors while still offering the highest-performing detection technology.
  • Enhance your ability to resolve large unit cells, twins or incommensurate lattices when you select the optional motorized variable beam slit in order to alter divergence to adapt the source to your sample’s requirements.


five starsRead what our customers say about the XtaLAB Synergy-S


 

Single or dual microfocus X-ray diffractometer for all your crystallography needs

A fast and agile single crystal X-ray diffractometer for small molecule 3D structure analysis

XtaLAB Synergy-S

With your success utmost in our minds, we have developed the XtaLAB Synergy-S X-ray diffractometer for single crystal X-ray diffraction. Using a combination of leading-edge components and user-inspired software tied together through a highly parallelized architecture, the XtaLAB Synergy-S produces fast, accurate data in an intelligent fashion. The system is based around the PhotonJet-S series of microfocus X-ray sources that optionally incorporate continuously variable divergence slits. These third-generation sources have been designed to maximize X-ray photons at the sample by using a combination of new optics, new longer-life tubes and an improved alignment system. PhotonJet-S sources are available in Cu, Mo or Ag wavelengths in either a single or dual source configuration. The XtaLAB Synergy-S single crystal X-ray diffractometer comes with a kappa goniometer that incorporates fast motor speeds and a unique telescopic two-theta arm to provide total flexibility for your diffraction experiment. The system is also equipped with your choice of HPC hybrid photon counting detectors, the HyPix-6000HE or the large theta coverage detectors: HyPix-Arc 100° or HyPix-Arc 150°.

In some settings, there is a desire to share instrument resources across different research groups.  The XtaLAB Synergy-S in a dual-source configuration is the perfect system to be shared between protein crystallographers and chemical crystallographers: a Mo source will give the chemical crystallographers the wavelength necessary to reduce absorption from heavier elements and a Cu source, with optional continuously variable divergence slits, will give the protein crystallographer the functionality necessary to resolve large unit cells.

HyPix Detectors

Rigaku’s own HyPix family of detectors use solid state pixel array technology to enable direct X-ray photon detection and counting. Direct X-ray photon detection means that X-ray photons are counted instantaneously as they arrive at the detector. There is no conversion to visible light by a scintillator so the energy of the photon can be assessed at moment of detection. This leads to essentially noise free images. The HyPix detectors feature a 100 Hz frame rate which allows for data fine slicing even at the fastest goniometer speeds.  The HyPix detectors incorporate dual counters enabling several modes of operation. Rapid alternating counter electronics (RACE) technology enables the 100 Hz zero dead time mode, ensures that no pixel is blind for more than a few nanoseconds during exposure to X-rays. The high dynamic range mode combines the counters to offer a massive 31-bit counter depth. Dual thresholding offers differential modes and selective signal suppression. 

PhotonJet-S

The XtaLAB Synergy-S is defined by its new PhotonJet-S X-ray source.  The PhotonJet-S sources provide almost double the flux for all three target types (Mo, Cu, Ag) compared to the previous generation. For the best data quality, it is important to ensure any source provides highly reproducible flux frame after frame. As tube temperature changes, so does the X-ray flux reaching your sample. Controlling the temperature of our sources using closed-circuit water cooling offers the best solution for both consistent and high performance and reliability in a completely standalone package. 

Beam Conditioning

Where overlapping peaks are a concern, e.g. large unit cells, proteins, twinned or incommensurate, high beam divergence is undesirable. On PhotonJet sources, a software controlled, motorized variable beam slit is available as an option to alter divergence to adapt the source to your sample’s requirements. For those samples where intensity matters most, the slit can be fully opened giving the highest flux. For those where peak sharpness and overlap are factors, the beam can be limited to a divergence anywhere between 1 to 10 mrad.

CrysAlisPro v40

The XtaLAB Synergy-S comes complete with CrysAlisPro, our user-inspired data collection and data processing software for single crystal analysis. Designed around an easy-to-use graphical user interface, CrysAlisPro can be operated under fully automatic, semi-automatic or manual control. CrysAlisPro combines automated crystal screening, the fastest and most accurate strategy software available, concurrent data reduction and automatic small molecule structure solution. Visual feedback is provided for each step with clear, color-coded guidance so that both novices and experts can collect high-quality data in the shortest time possible.

CrysAlisPro can be operated in either a protein or small molecule dedicated workflow.  Popular third-party protein data processing packages can easily process diffraction data if desired.

AutoChem

AutoChem is the ultimate productivity tool for small molecule chemists, offering fast, fully automatic structure solution and refinement during data collection. Developed in collaboration with OlexSys Ltd (Durham University, UK), AutoChem works in conjunction with Olex² where more advanced structure solution and refinement functionality exists. AutoChem is seamlessly integrated within CrysAlisPro and forms an integral part of our ‘What is this?’ feature. The ‘What is this?’ feature gives you structures quickly and ensures you are not wasting time collecting full datasets on known samples or starting materials. It is an alternative pre-experiment option, which is used to plan your full data collections.

Specifications and features
Product name XtaLAB Synergy-S
Core attributes Single or dual microfocus sealed tube X-ray source diffractometer with hybrid pixel array detector and kappa goniometer
Detectors HyPix-6000HE or optionally the large theta coverage detectors HyPix-Arc 100° or HyPix-Arc 150°
X-ray source PhotonJet-S X-ray source with new microfocus sealed tube that incorporates a new mirror design and new alignment hardware. Three target types are available (Mo, Cu, Ag).
Goniometer Fast kappa geometry goniometer that allows data collection scan speeds of up to 10°/sec.
Accessories Oxford Cryostream 800, Oxford Cobra, XtaLAB Synergy FLOW robotic system, XtalCheck-S, High Pressure Kit, and Element Analyzer.
Computer External PC, MS Windows® OS
Core dimensions 1300 (W) x 1875 (H) x 850 (D) mm
Mass  550 kg (core unit)
Power requirements 1Ø, 90-130V 15A or 180-260V 4A

Video for XtaLAB Synergy-S diffractometer

Options and Accessories

The following accessories are available for this product
HyPix-Arc 150°

The HyPix-Arc 150° is an optional, unique curved Hybrid Photon Counting (HPC) X-ray detector for single crystal diffraction applications.

HyPix-Arc 100°

A curved single crystal X-ray diffraction detector based on direct X-ray detection technology with a higher 2θ range compared to a flat detector.

Oxford Cryostream 800

The 800 Series Cryostream is the most robust, efficient and user-friendly liquid nitrogen based low temperature system available today. Specific features include a superior laminar flow system, meaning virtually zero risk of icing, extremely quiet running and a fast-start system resulting in a cool-down time to 100K of just 20 minutes.

Oxford Cobra

The Oxford Cobra is the non-liquid nitrogen Cryostream. Combining the efficiency of a Cryostream with the advantages of a non-liquid system, the Cobra offers the ultimate solution for both macromolecular and small molecule crystallography.

XtalCheck-S

The XtalCheck-S system includes software that facilitates both visual and diffraction imaging of crystallization experiments. With the XtalCheck-S system, one can easily survey many crystallization experiments by eliminating the need to harvest and cryo-cool samples. Moreover, one can perform serial crystallography experiments, by collecting data from multiple crystals, to achieve complete data sets that can be used for structure solution, as well as perform powder data collection from samples mounted in the crystallization wells.

High Pressure Kit

Accommodating the vast majority of commercially available and custom high pressure cells the high pressure kit creates a sample space with an 8 cm diameter. It’s easy to switch between high pressure and standard mode and with powerful high-pressure software tools to aid with data analysis and processing, high pressure diffraction experiments have never been easier.


*Please check with your local sales person if your DAC is supported

XtaLAB Synergy Flow

Robotic sample changer to provide unattended data acquisition, enhanced productivity and standardized workflow to your research environment.

ELement ANalyzer

The ELement ANalyzer is a state-of-the-art attachment that allows us to obtain qualitative information on elements in a single crystal at the same time as X-ray diffraction data collection for a single crystal structural analysis. By measuring the X-ray fluorescence spectrum emitted during X-ray diffraction experiments with the ELement ANalyzer, it becomes possible to perform elemental analysis on a single grain of crystal. The ELement ANalyzer can be used for confirmation the presence of central metal(s) in a mononuclear or polynuclear complex or solvent in a crystal for small molecule X-ray crystallography. There is a broad range of possible applications of the ELement ANalyzer in scientific fields.

Intelligent Goniometer Head (IGH)

The smallest detachable motorized goniometer head on the market.

XtaLAB Synergy-S Testimonials

Chemical Analysis Facility, University of Reading

"We’d have no hesitation in recommending the Synergy system. The combination of excellent hardware and software is a powerful one, and our close working relationship with Rigaku gives us confidence that we’ve made a sound choice that will serve us well for the foreseeable future.”

Crystallography Lab at Emory University

"I underestimated the impact a new system would have on the workflow and our ability to analyse multiple samples. It has allowed us to remain competitive, and to be able to provide the necessary service support for research groups in the department.”

Natural History Museum, University of Oslo

"After six months I am impressed with the instrument’s performance, and also the software. Furthermore, in my dealings with Rigaku, I have always been listened to as a customer and have received quick responses, something I have lacked with other companies."

X-ray Diffraction Facility at Cornell University

"My decision was ultimately cemented by doing a demo of the instrument and I would recommend that anyone considering making a purchase do one, either in person or virtually. I absolutely would recommend my new system – the combination of speed, quality and design has transformed the way that we are doing research in the facility."

University of Southern Denmark

"With our new instrument we were able to remove the backlog for data collections through rapid collection of good quality crystals. It has also permitted realistic use of single crystal crystallography as in integral part of undergraduate laboratory classes."

Texas Tech University

"The thing that really stuck out in our minds was the number of Synergy users that had experiences with other instrument companies and how impressed they were with both the instrument and the level of customer service that Rigaku was providing.   ”

Papers published using the XtaLAB Synergy-S

  1. Matthew A. Baker, Josué Ayuso-Carrillo, Martin R. M. Koos, Samantha N. MacMillan, Anthony J. Varni, Roberto R. Gil, Kevin J. T. Noonan A robust nickel catalyst with an unsymmetrical propyl-bridged diphosphine ligand for catalyst-transfer polymerization Polymer Journal 2020 52(1) , 83-92
  2. Penghua Shu, Mengyuan Sun, Junping Li, Lingxiang Zhang, Haichang Xu, Yueyue Lou, Zhiyu Ju, Xialan Wei, Wenming Wu, Na Sun Chemical constituents from Ginkgo biloba leaves and their cytotoxicity activity Journal of Natural Medicines 2020 74(1) , 269-274
  3. Shuai Shao, Habtom B. Gobeze, Venugopal Bandi, Christiane Funk, Brian Heine, Maddie J. Duffy, Vladimir Nesterov, Paul A. Karr, Francis D'Souza Triplet BODIPY and AzaBODIPY Derived Donor-acceptor Dyads: Competitive Electron Transfer versus Intersystem Crossing upon Photoexcitation ChemPhotoChem 2020 4(1) , 68-81
  4. Prince Ravat, Olivier Blacque, Michal Juríček Benzo[cd]triangulene: A Spin 1/2 Graphene Fragment The Journal of Organic Chemistry 2020 85(1) , 92-100
  5. Konstantin S. Usachev, Bulat F. Fatkhullin, Evelina A. Klochkova, Aynur K. Miftakhov, Alexander A. Golubev, Aidar G. Bikmullin, Liliya I. Nurullina, Natalia S. Garaeva, Daut R. Islamov, Azat G. Gabdulkhakov, Natalia V. Lekontseva, Svetlana V. Tishchenko, Vitaly A. Balobanov, Iskander Sh. Khusainov, Marat M. Yusupov, Shamil Z. Validov Dimerization of long hibernation promoting factor from Staphylococcus aureus: Structural analysis and biochemical characterization Journal of Structural Biology 2020 209(1) , 107408
  6. Karolina Matuszek, R. Vijayaraghavan, Craig M. Forsyth, Surianarayanan Mahadevan, Mega Kar, Douglas R. MacFarlane Pyrazolium Phase-Change Materials for Solar-Thermal Energy Storage ChemSusChem 2020 13(1) , 159-164
  7. Rebekah N. Duffin, Victoria L. Blair, Lukasz Kedzierski, Philip C. Andrews Anti-leishmanial activity and cytotoxicity of a series of tris-aryl Sb(V) mandelate cyclometallate complexes Journal of Inorganic Biochemistry 2020 203, 110932
  8. Brendan L. Murphy, Sierra C. Marker, Valencia J. Lambert, Joshua J. Woods, Samantha N. MacMillan, Justin J. Wilson Synthesis, characterization, and biological properties of rhenium(I) tricarbonyl complexes bearing nitrogen-donor ligands Journal of Organometallic Chemistry 2020 907, 121064
  9. Sajjad Soltani, Kamran Akhbari, Jonathan White Synthesis, crystal structure and antibacterial activity of a homonuclear nickel(II) metal-organic nano supramolecular architecture Polyhedron 2020 176, 114301
  10. Poornasha K. Mohabeer, Bronte Carr, Muhammad Hanif, Christian Hartinger, Tatiana Groutso, Rebecca E. Jelley, Tilo Söhnel, Allan G. Blackman Synthesis, structure and fluxionality of Co(III) complexes containing chelated sulfate Polyhedron 2020 176, 114303
  11. Bang-Ke Guo, Fei Yang, Ya-Qi Wang, Qiong Wei, Li Liu, Xin-Xin Zhong, Lei Wang, Jian-Kang Gong, Fa-Bao Li, Wai-Yeung Wong, Khalid A. Alamry, Yi Zhao Efficient TADF-OLEDs with ultra-soluble Copper(I) halide complexes containing non-symmetrically substituted bidentate phosphine and PPh3 ligands Journal of Luminescence 2020 220, 116963
  12. Ce Wang, Zheng Yin, Zhao Cheng, Wei-Min Ma, Xi-Yao Li, Xiao-Ting Hu, Rong Shi, Ao-Wei Chen, Yang-Min Ma A series of anionic MOFs with cluster-based, pillared-layer and rod-spacer motifs: near-sunlight white-light emission and selective dye capture CrystEngComm 2020 22(5) , 878-887
  13. Yaping Tao, Ligang Han, Andong Sun, Kexi Sun, Qian Zhang, Wanqiang Liu, Jianbin Du, Zhaojun Liu Crystal Structure and Computational Study on Methyl-3-Aminothiophene-2-Carboxylate Crystals 2020 10(1) ,
  14. Sang Loon Tan, Edward R. T. Tiekink N,N'-Bis(pyridin-3-ylmethyl)ethanediamide monohydrate: crystal structure, Hirshfeld surface analysis and computational study Acta Cryst. E 2020 76(1) , 25-31
  15. Sang Loon Tan, Edward R. T. Tiekink The 1:2 co-crystal formed between N,N'-bis(pyridin-4-ylmethyl)ethanediamide and benzoic acid: crystal structure, Hirshfeld surface analysis and computational study Acta Cryst. E 2020 76(1) , 102-110
  16. Sindija Lapcinska, Pavel Arsenyan Selenocystine peptides performance in 5-endo-dig reactions Eur. J. Org. Chem. 2020
  17. Farah Natasha Haezam, Normah Awang, Nurul Farahana Kamaludin, Mukesh M. Jotani, Edward R. T. Tiekink (N,N-Diallyldithiocarbamato-[kappa]2S,S')triphenyltin(IV) and bis(N,N-diallyldithiocarbamato-[kappa]2S,S')diphenyltin(IV): crystal structure, Hirshfeld surface analysis and computational study Acta Cryst. E 2020 76(2) , 167-176
  18. Takahiro Asada, Yoichi Hoshimoto, Takahiro Kawakita, Takuya Kinoshita, Sensuke Ogoshi Axial Chirality around N–P Bonds Induced by Complexation between E(C6F5)3 (E = B, Al) and an N-Phosphine Oxide-Substituted Imidazolinylidene: A Key Intermediate in the Catalytic Phosphinoylation of CO2 The Journal of Organic Chemistry 2020
  19. Joshua W. Prybil, Rodney Wallace, Alexandra Warren, Jordan Klingman, Romane Vaillant, Michael B. Hall, Xin Yang, William W. Brennessel, Robert M. Chin Silylation of Pyridine, Picolines, and Quinoline with a Zinc Catalyst ACS Omega 2020 5(3) , 1528-1539
  20. Gev Dovrat, Marie-Claire Illy, Claude Berthon, Ana Lerner, Moshe Mintz, Eric Maimon, Radion Vainer, Yeshayahu Ben-Elyiahu, Yulia Moiseev, Philippe Moisy, Armand Bettelheim, Israel Zilbermann On the aqueous chemistry of the U-IV-DOTA complex Chem. Eur. J. 2020
  21. Kristīne Krūkle-Bērziņa, Sergey Belyakov, Anatoly Mishnev, Kirill Shubin Stability and Phase Transitions of Nontoxic γ-Cyclodextrin-K+ Metal-Organic Framework in Various Solvents Crystals 2020 10(1) ,
  22. Shangxiong Huangfu, Gawryluk Dariusz Jakub, Xiaofu Zhang, Olivier Blacque, Pascal Puphal, Ekaterina Pomjakushina, Fabian O. von Rohr, and Andreas Schilling. Anisotropic character of the metal-to-metal transition in Pr4NiO arXiv: 2020 2001.05916
  23. Mao Arita, Soichi Yokoyama, Haruyasu Asahara, Nagatoshi Nishiwaki Three Step Synthesis of Fully and Differently Arylated Pyridines Eur. J. Org. Chem. 2020, 466-474
  24. Sang Loon Tan, Edward R. T. Tiekink Crystal structure, Hirshfeld surface analysis and computational study of the 1:2 co-crystal formed between N,N'-bis(pyridin-4-ylmethyl)ethanediamide and 4-chlorobenzoic acid Acta Cryst. E 2020 76(2) , 245-253
  25. Alasdair I. McKay, Weam A. O. Altalhi, Lachlan E. McInnes, Milena L. Czyz, Allan J. Canty, Paul S. Donnelly, Richard A. J. O’Hair Identification of the Side Products That Diminish the Yields of the Monoamidated Product in Metal-Catalyzed C–H Amidation of 2-Phenylpyridine with Arylisocyanates The Journal of Organic Chemistry 2020
  26. Michael Wörle, Christoph P. Guntlin, Luzia Gyr, Moulay T. Sougrati, Charles-Henri Lambert, Kostiantyn V. Kravchyk, Renato Zenobi, Maksym V. Kovalenko Structural Evolution of Iron(III) Trifluoroacetate Upon Thermal Decomposition: Chains, Layers and Rings Chemistry of Materials 2020
  27. Yang Yang, Allan J. Canty, Alasdair I. McKay, Paul S. Donnelly, Richard A. J. O’Hair Palladium-Mediated CO2 Extrusion Followed by Insertion of Isocyanates for the Synthesis of Benzamides: Translating Fundamental Mechanistic Studies To Develop a Catalytic Protocol Organometallics 2020
  28. Tate O. Engstrand, Kaya Wei, Ryan Baumbach, Yan Xin, Susan E. Latturner Structural Disorder in Intermetallic Boride Pr21M16Te6B30 (M = Mn, Fe): A Transition Metal Cluster and Its Evil Twin Inorganic Chemistry 2020

  1. Grzegorz Mlostoń, Małgorzata Celeda, Radomir Jasiński, Heinz Heimgartner Experimental and Computational Studies on Stepwise [3+2]-Cycloadditions of Diaryldiazomethanes with Electron-Deficient Dimethyl (E)- and (Z)-2,3-Dicyanobutenedioates Eur. J. Org. Chem. 2019, 422-431
  2. Michał Gacki, Karolina Kafarska, Anna Pietrzak, Izabela Korona-Glowniak, Wojciech M. Wolf Synthesis, characterisation, crystal structure and biological activity of metal(II) complexes with theophylline Journal of Saudi Chemical Society 2019 23(3) , 346-354
  3. Tan Yee Seng, Chun Hao Zhe, Jotani Mukesh M., Tiekink Edward R.T. Steric control of supramolecular association in structures of Zn(S2COR)2 with N,N′-bis(pyridin-4-ylmethyl)oxalamide Zeitschrift für Kristallographie - Crystalline Materials 2019 234, 165
  4. Koushik Sarkar, Parthasarathi Dastidar Rational Approach Towards Designing Metallogels From a Urea-Functionalized Pyridyl Dicarboxylate: Anti-inflammatory, Anticancer, and Drug Delivery Chem. Asian J. 2019 14(1) , 194-204
  5. Soichiro Akagi, Taishiro Horiguchi, Sho Fujii, Noboru Kitamura Terminal Ligand (L) Effects on Zero-Magnetic-Field Splitting in the Excited Triplet States of [{Mo6Br8}L6]2– (L = Aromatic Carboxylates) Inorganic Chemistry 2019 58(1) , 703-714
  6. Soichi Yokoyama, Nagatoshi Nishiwaki Fluorescence Behavior of Bis(cyanostyryl)pyrrole Derivatives Depending on the Substituent Position of Cyano Groups in Solution and in Solid State The Journal of Organic Chemistry 2019 84(3) , 1192-1200
  7. Takafumi Saito, Kenshu Fujiwara, Yoshihiko Kondo, Uichi Akiba, Takanori Suzuki Synthesis of the cyclohexene segment of portimine Tetrahedron Letters 2019 60(4) , 386-389
  8. Anjula M. Kosswattaarachchi, Lauren E. VanGelder, Olaf Nachtigall, Joshua P. Hazelnis, William W. Brennessel, Ellen M. Matson, Timothy R. Cook Transport and Electron Transfer Kinetics of Polyoxovanadate-Alkoxide Clusters Journal of The Electrochemical Society 2019 166(4) , A464-A472
  9. Sang Loon Tan, Edward R. T. Tiekink A 1:2 co-crystal of 2,2'-dithiodibenzoic acid and benzoic acid: crystal structure, Hirshfeld surface analysis and computational study Acta Cryst. E 2019 75(1) , 1-7
  10. Roger Townend, Ian E. Grey, W. Gus Mumme, Anthony R. Kampf, Malcolm P. Roberts, Robert W. Gable, and Rodney Dale. Amamoorite, CaMn2 Australian Journal of Mineralogy 2019 20(2) , 7
  11. Martin Babor, Philipp P. Nievergelt, Jan Cejka, Vit Zvonicek, Bernhard Spingler Microbatch under-oil salt screening of organic cations: single-crystal growth of active pharmaceutical ingredients IUCrJ 2019 6(1) , 145-151
  12. Rajagopal Rajesh, E. S. Sella, Olivier Blacque, Kunjanpillai Rajesh Crystal structure of a new 2,6-bis(imino)pyridine derivative: (1E,1'E)-1,1'-(pyridine-2,6-diyl)bis[N-(4-chlorophenyl)ethan-1-imine] Acta Cryst. E 2019 75(2) , 115-118
  13. Yi Jiun Tan, Yee Seng Tan, Chien Ing Yeo, Jactty Chew, Edward R.T. Tiekink In vitro anti-bacterial and time kill evaluation of binuclear tricyclohexylphosphanesilver(I) dithiocarbamates, {Cy3PAg(S2CNRR′)}2 Journal of Inorganic Biochemistry 2019 192, 107-118
  14. Jieming Zhen, Weiran Zhou, Muqing Chen, Bairu Li, Lingbo Jia, Mingtai Wang, Shangfeng Yang Pyridine-functionalized fullerene additive enabling coordination interactions with CH3NH3PbI3 perovskite towards highly efficient bulk heterojunction solar cells J. Mater. Chem. A 2019 7(6) , 2754-2763
  15. Monika Pitucha, Zbigniew Karczmarzyk, Marta Swatko-Ossor, Waldemar Wysocki, Maciej Wos, Kamil Chudzik, Grazyna Ginalska, Andrzej Fruzinski Synthesis, In Vitro Screening and Docking Studies of New Thiosemicarbazide Derivatives as Antitubercular Agents Molecules 2019 24(2) ,
  16. Muhammad O. Ali, John C. Lasseter, Remigiusz Żurawiński, Anna Pietrzak, Jacek Pecyna, Jakub Wojciechowski, Andrienne C. Friedli, Damian Pociecha, Piotr Kaszyński Thermal and Photophysical Properties of Highly Quadrupolar Liquid-Crystalline Derivatives of the [closo-B12H12]2− Anion Chem. Eur. J. 2019 25(10) , 2616-2630
  17. A. Paden King, Hendryck A. Gellineau, Samantha N. MacMillan, Justin J. Wilson Physical properties, ligand substitution reactions, and biological activity of Co(iii)-Schiff base complexes Dalton Trans. 2019 48(18) , 5987-6002
  18. Henry C. Neal, Harsha Tamtam, Bradley W. Smucker, Volodymyr V. Nesterov Redetermination of poly[di-[mu]3-iodido-[[mu]-1,2-trans-(pyridin-4-yl)ethene-[kappa]2N:N']dicopper(I)] IUCrData 2019 4(1) , x190122
  19. Wiebke Drescher (née Oschmann), Corinna Borner, Daniel J. Tindall, Christian Kleeberg Exploring unsymmetrical diboranes(4) as boryl ligand precursors: platinum(ii) bis-boryl complexes RSC Adv. 2019 9(7) , 3900-3911
  20. Patience B. Girigiri, Stephanie H. Carpenter, William W. Brennessel, Michael L. Neidig Crystal structure of bromidopentakis(tetrahydrofuran-[kappa]O)magnesium bis[1,2-bis(diphenylphosphanyl)benzene-[kappa]2P,P']cobaltate(-1) tetrahydrofuran disolvate Acta Cryst. E 2019 75(2) , 304-307
  21. Robert Malmberg, Michael Bachmann, Olivier Blacque, Koushik Venkatesan Thermally Robust and Tuneable Phosphorescent Gold(III) Complexes Bearing (N^N)-Type Bidentate Ligands as Ancillary Chelates Chem. Eur. J. 2019 25(14) , 3627-3636
  22. Jolanta Prywer, Lesław Sieroń, Agnieszka Czylkowska Struvite Grown in Gel, Its Crystal Structure at 90 K and Thermoanalytical Study Crystals 2019 9(2) ,
  23. I. Chien Yeo, H. Ainnul Azizan, R.T. Edward Tiekink 4-(4-Chlorophenyl)-4,5-dihydro-1H-1,2,4-triazole-5-thione Molbank 2019,
  24. Takuya Taniguchi, Hiroyasu Sato, Yuki Hagiwara, Toru Asahi, Hideko Koshima Photo-triggered phase transition of a crystal Communications Chemistry 2019 2(1) , 19
  25. Chilaluck Konkankit, Brett A. Vaughn, Samantha N. MacMillan, Eszter Boros, Justin J. Wilson Combinatorial Synthesis to Identify a Potent, Necrosis-Inducing Rhenium Anticancer Agent Inorganic Chemistry 2019 58(6) , 3895-3909
  26. William Henderson, Jesse C. Thomas, Obinna C. Okpareke, Edward R.T. Tiekink Synthesis, structural and mass spectrometric investigations of pyridinium bis(thiosalicylato)mercurate(II) Inorganica Chimica Acta 2019 490, 104-111
  27. Felicia Phei Lin Lim, Khai Ching Tan, Giuseppe Luna, Edward R.T. Tiekink, Anton V. Dolzhenko A new practical synthesis of 3-amino-substituted 5-aminopyrazoles and their tautomerism Tetrahedron 2019 75(15) , 2314-2321
  28. Felicia Phei Lin Lim, Giuseppe Luna, Khai Ching Tan, Edward R.T. Tiekink, Anton V. Dolzhenko A synthesis of new 7-amino-substituted 4-aminopyrazolo[1,5-a][1,3,5]triazines via a selective three-component triazine ring annulation Tetrahedron 2019 75(15) , 2322-2329
  29. Jinhua Li, Yu-Mei Lin, Hong Zhang, Yuan Chen, Zhenyang Lin, Haiping Xia Access to Metal-Bridged Osmathiazine Derivatives by a Formal [4+2] Cyclization Chem. Eur. J. 2019 25(19) , 5077-5085
  30. I. Chien Yeo, R. T. Edward Tiekink 1-[N-Methyl-N-(Phenyl)amino]-3-(4-Methylphenyl)Thiourea Molbank 2019,
  31. Atsushi Kobayashi, Momoko Fujii, Yasuhiro Shigeta, Masaki Yoshida, Masako Kato Quantitative Solvent-Free Thermal Synthesis of Luminescent Cu(I) Coordination Polymers Inorganic Chemistry 2019 58(7) , 4456-4464
  32. Ren A. Wiscons, Veaceslav Coropceanu, Adam J. Matzger Quaternary Charge-Transfer Solid Solutions: Electronic Tunability through Stoichiometry Chemistry of Materials 2019 31(17) , 6598-6604
  33. Yusuke Takahashi, Takuya Uehara, Chihiro Matsuhashi, Minoru Yamaji, Toshiki Mutai, Isao Yoshikawa, Hirohiko Houjou, Kota Kitagawa, Tomoyoshi Suenobu, Shojiro Maki, Takashi Hirano Spectroscopic properties of push-pull 2-(4-carboxyphenyl)-6-dimethylaminobenzothiazole derivatives in solution and the solid state Journal of Photochemistry and Photobiology A: Chemistry 2019 376, 324-332
  34. Sang Loon Tan, Edward R. T. Tiekink A 1:1:1 co-crystal solvate comprising 2,2'-dithiodibenzoic acid, 2-chlorobenzoic acid and N,N-dimethylformamide: crystal structure, Hirshfeld surface analysis and computational study Acta Cryst. E 2019 75(4) , 475-481
  35. Abed Yousefi, Seyyed Javad Sabounchei, Seyed Hamed Moazzami Farida, Roya Karamian, Nosrat Rahmani, Robert W. Gable Different properties of P,C-donor Pd(II) and Pt(II); spectroscopic and X-ray analysis, catalytic potential and anti-proliferative potency Journal of Organometallic Chemistry 2019 890, 21-31
  36. Brittney Petel, Alex A. Fertig, Michela L. Maiola, William W. Brennessel, Ellen M. Matson Controlling Metal-to-Oxygen Ratios via M═O Bond Cleavage in Polyoxovanadate Alkoxide Clusters Inorganic Chemistry 2019 58(16) , 10462-10471
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